Method for Determining Identity:Proton NMR (CD3OD) and MS
TLC Conditions:SiO2; Dichloromethane: Methanol: Ammonium Hydroxide (9 :1 : 0.2); Visualized with UV and KMnO4 (single spot; Rf= 0.45).
Storage and Stability:Store under inert atmosphere at 4°C. Caution: Hygroscopic. For maximum recovery of product, centrifuge the original vial prior to removing the cap.