Method for Determining Identity:Proton NMR (CD3OD), C-13 NMR (CD3OD), 19-F NMR (CD3OD) and MS
TLC Conditions:SiO2; Dichloromethane : Methanol (8 : 2). Visualized with UV and AMCS (single spot; Rf=0.45)
Storage and Stability:Store at -20°C under inert atmosphere. Caution: Hygroscopic. For maximum recovery of product, centrifuge the original vial prior to removing the cap.